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Working with air conditioner service station -> 2.13 Filling contaminated refrigerant in a recycling cylinder for analysis, processing or disposal for Your Volkswagen Scirocco SUV Third Generation (2008-2017)

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Air conditioning systems with refrigerant R1234yf - General information - Edition 07.2017  
Note  
Replacement compressors clokntain a certain specified quantity  
of refrigerant oil. On vehicles with two evaporators, a certain  
amount of refrigerant oil may also have to be filled in the circuit  
if necessary ⇒ Heating, air conditioning; Rep. gr. 00 ; Tech‐  
nical data; Refrigerant oil .  
If the air conditioner compressor does not need to be renewed,  
replenish the refrigerant oil accordingly up to the prescribed fill  
level (empty or flush refrigerant oil and pour the prescribed  
volume back into the air conditioner compressor or refrigerant  
circuit) ⇒ “1.5 Renewing components”, page 79 and ⇒ Heat‐  
ing, air conditioning; Rep. gr. 00 ; Technical data; refrigerant  
oil .  
– Completely reassemble the refrigerant circuit again ⇒ Heat‐  
ing, air conditioning; Rep. gr. 87 ; Refrigerant circuit; System  
overview - refrigerant circuit (vehicle-specific workshop man‐  
ual).  
– Evacuate and charge the refrigerant circuit in accordance with  
the specifications  
⇒ “2.5 Evacuating refrigerant circuit”, page 140 ,  
⇒ “2.6 Charging refrigerant circuit”, page 146 and ⇒ Heating,  
air conditioning; Rep. gr. 00 ; Technical data .  
– Bring the air conditioning system into operation in the prescri‐  
bed manner ⇒ Heating, air conditioning; Rep. gr. 87 ; Refrig‐  
erant circuit; Bringing air conditioning system into operation  
after charging refrigerant circuit (vehicle-specific workshop  
manual) and  
⇒ “2.7 Bringing air conditioning system into service after  
charging”, page 149  
2.13  
Filling contaminated refrigerant in a re‐  
cycling cylinder for analysis, processing  
or disposal  
⇒ “2.13.1 Filling contaminated refrigerant in a recycling cylinder  
using technical equipment”, page 161  
⇒ “2.13.2 Filling undercooled contaminated refrigerant in a recy‐  
cling cylinder”, page 164  
2.13.1  
Filling contaminated refrigerant in a re‐  
cycling cylinder using technical equip‐  
ment  
Note  
Some manufacturers may provide accessory devices (extract‐  
ing or disposal units) that they claim to be approved for the  
extraction of gases of unknown composition. These devices,  
however, have not been tested or approved by Volkswagen  
so that we cannot draw any conclusions about their operation  
or suitability.  
In order to be filled into an evacuated recycling cylinder without  
any auxiliary equipment, the contaminated refrigerant must be  
supercooled. The corresponding procedure has been ap‐  
proved by Volkswagen and described accordingly  
⇒ page 164 .  
2. Working with air conditioner service station  
161  
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Air conditioning systems with refrigerant R1234yf - General information - Edition 07.2017  
CAUTION  
Risk of explosion if non-approved equipment is used  
Refrigerant of unknown composition may expand due to a  
chemical reaction or overheating causing the used device to  
burst.  
lk  
– Make sure to use only devices and accessories that have  
been authorised and approved by the manufacturer for be‐  
ing suitable for operation with gases of unknown composi‐  
tion in accordance with the relevant rules and regulations.  
– Always read the owner's manual of these devices before  
using them.  
– Make sure to comply with all instructions given in the re‐  
spective owner's manual when using the devices.  
CAUTION  
Risk of explosion from overfilling refrigerant reservoirs.  
Refrigerant can expand and cause reservoirs to burst if they are  
overfilled.  
– Use a refrigerant tank with safety valve.  
– Never exceed the permissible fill level of the refrigerant tank.  
CAUTION  
Chemical reactions from contaminated refrigerant. Mixing  
gases of unknown composition can cause different chemical  
reactions.  
Risk of injuries.  
– Never mix together refrigerants of different origins.  
Extract refrigerant of unknown composition from refrigerant circuit  
and collect it in a recycling cylinder.  
– Connect the extracting and charging unit to the refrigerant cir‐  
cuit of the vehicle and to a recycling cylinder observing the  
corresponding owner's manual.  
– Operate the extracting and charging unit according the in‐  
structions in the corresponding owner's manual.  
– Monitor the extraction process using a suitable pressure  
gauge.  
Note  
You can use your own pressure gauge or the pressure gauge  
of the air conditioner service station to monitor the extraction  
process.  
As it will take some time until the entire contaminated refrig‐  
erant has been extracted from the refrigerant circuit, make  
sure that you do not switch off the extracting and charging unit  
until the refrigerant circuit has been drained completely. To be  
absolutely sure about this, watch the display of the connected  
pressure gauge.  
After the entire contaminated refrigerant has been extracted from  
the circuit:  
– Switch off unit.  
– Close the manual shut-off valve of the recycling cylinder.  
162  
Rep. gr.87 - Air conditioning system  
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Air conditioning systems with refrigerant R1234yf - General information - Edition 07.2017  
– Wait a certain amount of time (e.g. 20 minutes), then check if  
pressure started building up again in the vehicle’s refrigerant  
circuit.  
Note  
lk  
If pressure started building up in the refrigerant circuit due to  
evaporation of refrigerant, fill the refrigerant responsible for this  
increase in pressure into the recycling cylinder.  
– Remove the charge hose and adapter from the recycling cyl‐  
inder, and seal the connection of the recycling cylinder with  
the sealing cap.  
– The paperwork required for analysis, processing (or disposal)  
of contaminated refrigerant must be filled in completely (dis‐  
posal record, acceptance certificate etc.).  
Note  
All of the information and documents for analysis, processing  
(or disposal) can be obtained from your gas processing / gas  
disposal company.  
Included with the recycling cylinder is a form. Kindly fill this in  
accordingly and attach it to the recycling cylinder.  
If it is not possible to weigh the recycling cylinder before and  
after filling with contaminated refrigerant, the fill volume speci‐  
fied for the vehicle in question can be quoted as the amount  
of refrigerant that was filled in the recycling cylinder. This is  
permissible as only the amount of refrigerant from a vehicle is  
filled in a recycling cylinder.  
– Take the recycling cylinder to a suitable location for storage  
until it is ready to be collected by the gas processing / gas  
disposal company.  
– Fill out the data sheet for the recycling cylinder (R-cylinder) if  
the refrigerant is contaminated, and firmly attach it to the re‐  
cycling cylinder.  
Note  
In the “Other comments” section, details can be provided re‐  
garding e.g. who is to receive the analysis results and in which  
way.  
Example for recycling cylinder (R-cylinder) data sheet  
⇒ page 169 .  
– Evacuate the refrigerant circuit with the air conditioner service  
station for at least 1 hour  
⇒ “2.5 Evacuating refrigerant circuit”, page 140 .  
2. Working with air conditioner service station  
163  
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Air conditioning systems with refrigerant R1234yf - General information - Edition 07.2017  
Note  
Subsequent evacuation results in the last remnants of conta‐  
minated refrigerant, which could still be in the refrigerant oil,  
being removed at an absolute pressure of less than 10 mbar.  
If, after the unit has been switched off, a pressure that is higher  
than the maximum permissible pressure for the function  
“Evacuate” to be started on the air conditioner service station  
builds up in the refrigerant circuit, release this pressure (drain  
refrigerant) into the workshop extraction unit.  
The next steps depend on the complaint with the refrigerant  
circuit  
⇒ “2.3 Performing gas analysis of refrigerant”, page 134 .  
2.13.2  
Filling undercooled contaminated refrig‐  
erant in a recycling cylinder  
Note  
To ensure that the contaminated refrigerant is filled automat‐  
ically without supporting equipment into an evacuated recy‐  
cling cylinder, the cylinder must be supercooled.  
To cool down the evacuated recycling bottle, use an insulated  
container and dry ice.  
Dry ice is solid carbon dioxide (CO ) that changes from a solid  
2
lk  
directly to a gaseous state at -78°C.  
Most of the gases used as refrigerant have only a low vapour  
pressure at very low temperatures (less than 0.6 bar absolute  
pressure at -50°C). When an extremely cooled recycling cyl‐  
inder is connected to a refrigerant circuit, the refrigerant liq‐  
uefies in the cold recycling cylinder and the pressure in the  
refrigerant circuit drops below ambient pressure  
⇒ “6.1.3 Vapour pressure table for refrigerant”, page 17 .  
Commercially available recycling cylinders are usually made  
of common mild steel. These are not always suitable for low  
temperatures (down to -78°C in this case), which is why only  
recycling cylinders suitable for this application should be used  
and why the cylinder should be allowed to reach ambient tem‐  
perature slowly (e.g. by placing the insulated container with  
recycling cylinder in a secure, well-ventilated location where  
the dry ice can evaporate safely).  
Special tools and workshop equipment required  
♦ Extraction unit - VAS 581 007- ⇒ Electronic parts  
catalogue (ETKA)  
♦ At least 10 kg of commercially available dry ice (pellets or  
granules)  
♦ Evacuated recycling cylinder from gas supplier for contami‐  
nated R1234yf refrigerant, which is suitable for very low tem‐  
peratures (e.g. with a permissible fill capacity greater than  
3.0 kg).  
♦ Commercially available bottle adapter with seal (for connect‐  
ing charge hose to recycling bottle, internal W 21.8 x 1/14 LH  
left-hand thread and M 12 x 1.5-6G in accordance with SAE  
J639)  
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Air conditioning systems with refrigerant R1234yf - General information - Edition 07.2017  
♦ Commercially available charge hose for R1234yf refrigerant  
with seals (2m charge hose with external M12 x 1.5-6G thread  
in accordance with SAE J639)  
♦ Commercially available low-pressure service coupling in ac‐  
cordance with SAE J639  
Note  
Dry ice evaporates at ambient temperature even from the insu‐  
lated container (about 20 to 30% per day depending on the  
ambient conditions). Therefore, only order the dry ice once all of  
the necessary tools are ready and the measures can be per‐  
formed immediately after receipt of the dry ice (e.g. do not order  
the dry ice on a Friday if work is not going to be carried out at the  
weekend).  
CAUTION  
Risk of frost-bite and suffocation from dry ice.  
lk  
Frost-bite on the skin and other body parts possible and risk of  
suffocation in gaseous state.  
– Wear protective gloves.  
– Wear protective goggles.  
– Only work with dry ice in well ventilated areas.  
– Never work in or near cellars or other low lying areas.  
CAUTION  
Risk of explosion from incorrectly stored dry ice.  
As dry ice evaporates, pressure builds up in the container. Un‐  
suitable containers could burst.  
– Only transport and store dry ice in dedicated containers.  
Refilling refrigerant using a supercooled recycling cylinder  
All requisite tools, equipment and a sufficient quantity of dry  
ice ready  
– Remove seal on recycling cylinder and unscrew sealing cap  
from connection.  
2. Working with air conditioner service station  
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Air conditioning systems with refrigerant R1234yf - General information - Edition 07.2017  
Note  
Sealed recycling cylinders from your gas supplier usually  
come pre-evacuated.  
Should the recycling cylinder not be evacuated, evacuate it as  
necessary using a vacuum pump or an air conditioner service  
station .  
Recycling cylinders are clearly marked as such and, unlike  
refrigerant cylinders, do not have a non-return valve thereby  
making them suitable for filling.  
Recycling cylinders are designed for international use, which  
is why the “O” on the handwheel means “Open” (cylinder valve  
= open) and not “0” (zero = closed).  
If an absolute pressure greater than 100 mbar but less than  
900 mbar is measured in the recycling cylinder, evacuate the  
recycling cylinder using a vacuum pump (or an air conditioner  
service station ) (residual pressure less than 50 mbar)  
⇒ “2.5 Evacuating refrigerant circuit”, page 140 .  
If an absolute pressure greater than 900 mbar is measured in  
the recycling cylinder, this could be due to a number of rea‐  
sons. The manual shut-off valve was opened and not closed  
properly or the recycling cylinder had previously been used to  
store refrigerant and then was not evacuated properly  
⇒ “2.10 Emptying air conditioner service station”, page 154  
(evacuate recycling cylinder). The recycling cylinder is leaking  
(return the recycling cylinder to the supplier).  
lk  
– Connect a vacuum metre (or air conditioner service station )  
to the recycling cylinder.  
– Carefully open the manual shut-off valve of the recycling cyl‐  
inder to check the vacuum and then check the vacuum in the  
cylinder.  
– If necessary, evacuate the recycling cylinder with the air con‐  
ditioner service station .  
Note  
Should there be any air trapped in the recycling cylinder, it can  
be evacuated using an air conditioner service station for  
R1234yf. To do this, unscrew the low pressure service cou‐  
pling from the charge hose of the air conditioner service station  
and connect the charge hose directly to the recycling cylinder  
adapter for the extraction device (for R1234yf refrigerant) - dry  
ice box .  
If air is trapped in the recycling cylinder and there is no air  
conditioner service station for R1234yf available, the recycling  
cylinder can also be evacuated with an air conditioner service  
station for R134a using a relevant flushing container and  
adapter -VAS 6338/38- along with the charge hose from ex‐  
traction device (for R1234yf refrigerant) - dry ice box .  
Residual pressure in the recycling cylinder less than 10 mbar  
absolute pressure.  
166  
Rep. gr.87 - Air conditioning system  
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Air conditioning systems with refrigerant R1234yf - General information - Edition 07.2017  
Note  
Recycling cylinders are pre-evacuated by the supplier, though  
it is not always possible to ensure that the vacuum will remain  
intact in storage.  
To reliably determine the type and scope of the contamination  
of the refilled refrigerant during analysis of the contaminated  
refrigerant, the recycling cylinder must be evacuated before  
refilling to a residual pressure less than 50 mbar.  
– Switch off ignition.  
– Ensure that the workplace is well ventilated. Switch on addi‐  
tional workshop extraction systems if fitted.  
– Connect the charge hose with a suitable adapter to the evac‐  
uated recycling cylinder.  
CAUTION  
Risk of explosion from overfilling refrigerant reservoirs.  
Refrigerant can expand and cause reservoirs to burst if they are  
overfilled.  
– Use a refrigerant tank with safety valve.  
– Never exceed the permissible fill level of the refrigerant tank.  
lk  
Note  
Since contaminated refrigerant is only filled into a recycling  
cylinder from a vehicle in the following work routine, there is  
no danger of a recycling cylinder being overfilled with a fill vol‐  
ume exceeding 3.0 kg.  
If contaminated refrigerant is filled into a recycling cylinder e.g.  
from an air conditioner service station , measures must be  
taken to ensure that the recycling cylinder is not overfilled due  
to the larger volume. Use a recycling cylinder with an appro‐  
priate permissible fill capacity and when refilling ensure by  
means of weighing that the maximum permissible fill volume  
is not exceeded.  
CAUTION  
Chemical reactions from contaminated refrigerant. Mixing  
gases of unknown composition can cause different chemical  
reactions.  
Risk of injuries.  
– Never mix together refrigerants of different origins.  
2. Working with air conditioner service station  
167  
lk  
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Air conditioning systems with refrigerant R1234yf - General information - Edition 07.2017  
– Connect the service coupling for R1234yf refrigerant -5- to the  
charge hose -4-.  
– Connect the charge hose -4- with cylinder adapter -3- (and  
seal -2-) to the recycling cylinder -1-.  
– Place the spacer -6- in the insulated container -7-.  
– Cover the base of the insulated container -7- with dry ice.  
– Place the recycling cylinder -1- in the insulated container -7-  
extraction device (for R1234yf refrigerant) - dry ice box .  
– Pour the remainder of the dry ice in the insulated container  
-7-.  
– Cool down the recycling container -1- with dry ice (for approx.  
15 minutes).  
– Connect the recycling cylinder -1- via the service coupling  
-5- to the connection of the air conditioner service station (or  
the vehicle's refrigerant circuit).  
– Open the manual shut-off valve of the recycling cylinder -1-.  
Note  
Recycling cylinders are designed for international use, which is  
why the “O” on the handwheel means “Open” (cylinder valve =  
open) and not “0” (zero = closed).  
– Connect a pressure gauge to the refrigerant circuit (or use the  
pressure gauge of the air conditioner service station ) and  
check the pressure in the refrigerant circuit.  
– Carefully open the service coupling -5- on the charge hose for  
the recycling cylinder and allow the refrigerant to flow out  
slowly into the recycling cylinder -1-.  
– Wait until the refrigerant in the recycling cylinder -1- has liq‐  
uefied (watch the display on the connected pressure gauge).  
Note  
You can use your own pressure gauge or the pressure gauge  
of the air conditioner service station to monitor the extraction  
process.  
As soon as the displayed pressure is less than 0.3 bar after  
approx. 60 minutes, it is safe to assume that the whole refrig‐  
erant in the recycling cylinder is liquefied.  
Complete evaporation of the contaminated refrigerant from the  
refrigerant circuit takes some time. After 60 minutes, it is safe  
to assume that the whole refrigerant has evaporated.  
– Close the service coupling -5- and manual shut-off valve of the  
recycling cylinder -1-.  
– Remove the charge hose -4- and cylinder connecting piece  
-3- from the recycling cylinder -1- and close the recycling cyl‐  
inder with the cap.  
– The paperwork required for analysis, processing (or disposal)  
of contaminated refrigerant must be filled in completely (dis‐  
posal record, acceptance certificate etc.).  
168  
Rep. gr.87 - Air conditioning system  
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Air conditioning systems with refrigerant R1234yf - General information - Edition 07.2017  
Note  
All of the information and documents for analysis, processing  
(or disposal) can be obtained from your gas processing / gas  
disposal company.  
Included with the recycling cylinder is a form. Kindly fill this in  
accordingly and attach it to the recycling cylinder.  
If it is not possible to weigh the recycling cylinder before and  
after filling with contaminated refrigerant, the fill volume speci‐  
fied for the vehicle in question can be quoted as the amount  
of refrigerant that was filled in the recycling cylinder. This is  
permissible as only the amount of refrigerant from a vehicle is  
filled in a recycling cylinder.  
– Move the insulated box -7- with recycling cylinder -1- and dry  
ice to a secure, well ventilated area outside the building.  
– Open the lid of the insulated box -7- or remove and allow the  
dry ice to evaporate.  
Note  
Do not take the recycling cylinder -1- out of the insulated container  
-7- until the dry ice has evaporated and the recycling cylinder has  
adjusted to ambient temperature.  
– Remove the recycling cylinder -1- from the insulated container  
-7-.  
lk  
– Take the recycling cylinder -1- to a suitable location for storage  
until it is ready to be collected by the gas processing / gas  
disposal company.  
– Evacuate the refrigerant circuit with the air conditioner service  
station for at least 1 hour  
⇒ “2.5 Evacuating refrigerant circuit”, page 140 .  
Note  
Subsequent evacuation results in the last remnants of conta‐  
minated refrigerant, which could still be in the refrigerant oil,  
being removed at an absolute pressure of less than 10 mbar.  
The next steps depend on the complaint with the refrigerant  
circuit  
⇒ “2.3 Performing gas analysis of refrigerant”, page 134 .  
– Fill out the data sheet for the recycling cylinder (R-cylinder) if  
the refrigerant is contaminated and firmly attach it to the recy‐  
cling cylinder -1-.  
Note  
In the “Other comments” section, details can be provided regard‐  
ing e.g. who is to receive the analysis results and in which way.  
Example for recycling cylinder (R-cylinder) data sheet  
2. Working with air conditioner service station  
169